Laboratory Techniques in Organic Chemistry
Fourth Edition
Publication Date: March 01, 2014
Paperback ISBN: 9781464134227
Pages: 560
Laboratory Techniques in Organic Chemistry is the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds...
PART 1 Introduction to the Organic Laboratory
ESSAY The Role of the Laboratory1. Safety in the Laboratory
2. Green Chemistry
3. Laboratory Notebooks and Prelaboratory InformationPART 2 Carrying Out Chemical Reactions
ESSAY Learning to Do Organic Chemistry4. Laboratory Glassware
5. Measurements and Transferring Reagents
6. Heating and Cooling Methods
7. Setting Up Organic Reactions
8. Computational Chemistry PART 3 Basic Methods for Separation, Purification, and Analysis
ESSAY Intermolecular Forces in Organic Chemistry9. Filtration
10. Extraction
11. Drying Organic Liquids and Recovering Reaction Products
12. Boiling Points and Distillation
13. Refractometry
14. Melting Points and Melting Ranges
15. Recrystallization
16. Sublimation
17. Optical Activity and Enantiomeric AnalysisPART 4 Chromatography
ESSAY Modern Chromatographic Separations18. Thin-Layer Chromatography
19. Liquid Chromatography
20. Gas ChromatographyPART 5 Spectrometric Characterization Methods
ESSAY The Spectrometric Revolution21. Infrared Spectroscopy
22. Nuclear Magnetic Resonance Spectroscopy
23. 13C and Two-Dimensional NMR Spectroscopy
24. Mass Spectrometry
25. Ultraviolet and Visible Spectroscopy
26 . Integrated Spectrometry Problems
ESSAY The Role of the Laboratory1. Safety in the Laboratory
2. Green Chemistry
3. Laboratory Notebooks and Prelaboratory InformationPART 2 Carrying Out Chemical Reactions
ESSAY Learning to Do Organic Chemistry4. Laboratory Glassware
5. Measurements and Transferring Reagents
6. Heating and Cooling Methods
7. Setting Up Organic Reactions
8. Computational Chemistry PART 3 Basic Methods for Separation, Purification, and Analysis
ESSAY Intermolecular Forces in Organic Chemistry9. Filtration
10. Extraction
11. Drying Organic Liquids and Recovering Reaction Products
12. Boiling Points and Distillation
13. Refractometry
14. Melting Points and Melting Ranges
15. Recrystallization
16. Sublimation
17. Optical Activity and Enantiomeric AnalysisPART 4 Chromatography
ESSAY Modern Chromatographic Separations18. Thin-Layer Chromatography
19. Liquid Chromatography
20. Gas ChromatographyPART 5 Spectrometric Characterization Methods
ESSAY The Spectrometric Revolution21. Infrared Spectroscopy
22. Nuclear Magnetic Resonance Spectroscopy
23. 13C and Two-Dimensional NMR Spectroscopy
24. Mass Spectrometry
25. Ultraviolet and Visible Spectroscopy
26 . Integrated Spectrometry Problems
PART 6 Designing and Carrying out Organic Experiments
Essay Inquiry-Driven Lab Experiments
27. Designing Chemical Reactions
28. Using the Literature of Organic Chemistry
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